|
|
Calibration of Tungsten-Rhenium Thermocouple Based on High Temperature Blackbody Furnace |
NIU Xing-jun1,2,ZHANG Ting-ting2,FANG Li-de1,LU Xiao-feng2 |
1. School of Quality and Technical Supervision, Hebei University, Baoding, Hebei 071002, China
2. National Institute of Metrology, Beijing 100029, China |
|
|
Abstract A calibration method for high-temperature thermocouples, as tungsten-rhenium couples, was designed based on the high temperature blackbody furnace at the National Institute of Metrology(NIM). The axial uniformity of the optimally designed cavity in the temperature thermostat was measured less than 0.5℃ within 20mm depth. The radiance temperature difference between the selected cavity and the central one was less than 0.5℃. The calibration method based on the high temperature blackbody furnace was verified by Pt-10% Rh/Pt thermocouple. The calibration error from 800℃ to 1300℃ was less than 0.5℃, and the uncertainty was estimated 0.8~1.5℃, k=2. In the range of 800~1900℃, the electromotive force of tungsten-rhenium thermocouple from different manufactures was calibrated, and the uniformity of the wires before and after calibration was also tested. The calibration result showed that the relative error of the tungsten-rhenium thermocouple was kept within 1%, and the uncertainty was estimated 3.7~13.0℃, k=2 which was about 0.7%t in the relative uncertainty.
|
Received: 23 September 2021
Published: 18 May 2022
|
|
|
|
|
[1]陈宝有, 刘志超, 范玉佩, 等. 一种热电偶原位校准方法的研究 [J]. 计量技术, 2018(7): 57-59.
[2]魏树龙, 李时鑫, 蒋静, 等. 异型温度传感器的校准研究[J]. 计量技术, 2020(3):30-32.
[3]王魁汉, 李明华. “工业钨铼热电偶技术条件”新标准的编制与简介 [J]. 自动化仪表, 2017, 38(11): 62-67.
Wang K H, Li M H. Compilation and introduction of the new standard “technical conditions for industrial tungsten rhenium thermocouples” [J]. Automation instrument, 2017, 38(11): 62-67.
[4]罗拥军. 钨铼热电偶及其应用 [J]. 电子·仪器仪表用户, 1994(4): 6-9.
[5]Ogura H, Izuchi M, Tamba J. Stability of tungsten-rhenium thermocouples in the range from 0℃ to 1500℃ [J]. International Journal of Thermophysics, 2011, 32(11-12): 2420-2435.
[6]Ongrai O, Pearce J V, Machin G, et al. Self-calibration of a W/Re thermocouple using a miniature Ru-C (1954 C) eutectic cell [C]//AIP Conference Proceedings. Los Angeles, USA, 2013.
[7]王魁汉, 贺鸿业, 崔传孟. 钨铼热电偶在空气中的热电动势稳定性及其特性研究 [J]. 计量学报, 1997, 18(4): 2-5.
Wang K H, He H Y, Cui C M. Stability of thermoelectric force in air in air and its characteristics [J]. Acta Metrologica Sinica, 1997, 18(4): 2-5.
[8]刘丹英, 张贺, 吕国义, 等. 高温钨铼热电偶校准分析 [J]. 工业计量, 2015, 25(4): 13-15.
[9]李硕, 郭涛, 姚雅萱, 等. 热电材料塞贝克系数的不确定度评定[J]. 计量学报, 2021, 42(8): 1006-1011.
Li S, Guo T, Yao Y X, et al. The Uncertainty Evaluation of Seebeck Coefficient of Thermoelectric Materials[J]. Acta Metrologica Sinica, 2021, 42(8): 1006-1011.
[10]王喆, 余松林, 沈文杰, 等. 校准短型廉金属热电偶相关问题的研究 [J]. 计量学报, 2020, 41(6): 650-655.
Wang Z, Yu S L, Shen W J. Study on the problem of calibrating short low-quality thermocouple [J]. Acta Metrologica Sinica, , 2020, 41(6): 650-655.
[11]李朝, 刘戎, 侯运安. 均温块在热电偶校准中的应用探讨 [J]. 计测技术, 2018, 38(4): 17-19.
Li Z, Liu R, Hou Y A. Application of average thermocouple in thermocouple calibration [J]. Measurement technology, 2018, 38(4): 17-19.
[12]侯运安, 李朝. 热电偶检定炉温度场测试方法的探讨 [J]. 计测技术, 2013, 33(6): 76-78.
Hou Y A, Li Z. Discussion on Temperature Field Temperature Field Test Method [J]. Measurement technology, 2013, 33(06): 76-78.
[13]王浩, 侯素兰, 徐宏光, 等. 管式热电偶检定炉均匀温场的研究 [J]. 中国计量, 2010(10): 79-81.
[14]杨斌, 王惠龄. 热电偶不均匀性研究现状与进展 [J]. 仪器仪表用户, 2015, 22(3): 11-13.
Yang B, Wang H L. A Review of the Investigation of the Thermoelectric Inhomogeneity of Thermocouple Wires[J]. Instrumentation,2015, 22(3): 11-13.
[15]郑玮,汤磊,向明东. 高精度金-铂热电偶的制作和热电稳定性研究[J]. 计量学报, 2022, 43(2): 191-195.
Zheng W, Tang L, Xiang M D. The Research on Construction the High Precision Au/Pt Thermocouple and its Stability of Thermoelectric Character[J]. Acta Metrologica Sinica, 2022, 43(2): 191-195.
[16]刘红彦,张帅星,徐震震,等. 多区加热热电偶检定炉的温场研究[J]. 计量学报, 2022, 43(2): 228-234.
Liu H Y, Zhang S X, Xu Z Z, et al. Research on Temperature Uniformity of the Calibration Furnace with Multiple Calorifiers[J]. Acta Metrologica Sinica, 2022, 43(2): 228-234.
[17]李海燕. 热电偶不均匀性及实验测试方法的分析研究 [J]. 科技创新导报, 2012(24): 84.
[18]杨振华. 热电偶不均匀性分析及实验测试方法研究 [D]. 天津: 天津大学, 2010.
[19]郑玮, 杨振华, 向明东. 在液槽中测试热电偶不均匀性方法探索 [J]. 计量学报, 2013, 34(4): 356-359.
Zhang W, Yang Z H, Xiang M D. Exploration of testing thermocouple non-uniformity method in liquid tank [J]. Acta Metrologica Sinica, 2013, 34(04): 356-359.
[20]Machin G, Pearce J. Step change improvements in high-temperature thermocouple thermometry [C]//Proceedings of 2012 UKACC International Conference on Control. Cardiff, UK, 2012. |
|
|
|