|
|
Reliability Evaluation of Gas Dynamic Dilution Device |
WU Yu-tong1,BI Zhe1,YANG Yang-zhongfu2,MA Hao-miao1,WU Hai1,3 |
1. National Institute of Metrology,Beijing 100029,China
2. Chinese Society for Measurement,Beijing 100029,China
3. Zhengzhou Institute of Metrology, Zhengzhou, Henan 450001,China |
|
|
Abstract A dilution device was built based on mass flow controllers (MFC), and a high-precision CH4 spectrometer was used to evaluate the reliability of the gas dilution device. Experimental results showed that when the dilution ratio was 0.01~0.02, the relative error of the theoretical concentration of gas mixture produced by the device was not more than ±4%, and when the dilution ratio was 0.04~0.1, the relative error was within±0.5%. The accuracy of the dilution device was not so good when the dilution ratio was very small. The change of input gas pressure upstream of MFC had influence on its output gas flow. When the input pressure changed in the range of 0.2 ~ 0.6MPa, the variation range of MFC output gas flow was not more than 1%, resulting in the variation of standard gas concentration output by the dilution device was not more than 1%. When the input gas pressure changed in the range of (2~6)bar, the variation range of MFC output gas flow was not more than 1%. The input gas pressure variation could interfere with the diluted gas concentration generated by the dilution device, of which the influence was less than 1%. When using the dilution device to prepare standard gas, it is preferable to set the MFC in the range above 10% of its full scale, so as to ensure the reliability of the dilution device.
|
Received: 01 December 2020
Published: 15 July 2021
|
|
|
|
|
[1]潘素素, 张国城, 杨振琪, 等. 气体稀释装置检测方法初探 [J]. 计量技术, 2019, (12): 36-39.
Pan S S, Zhang G C, Yang Z Q, et al. A preliminary study on the detection method of gas dilution device [J]. Measurement Technique, 2019, (12): 36-39.
[2]李建鹏, 闫继伟, 许雪琼, 等. 质量流量控制器动态配气装置量值溯源方法分析 [J]. 工业计量, 2019, 29 (1): 40-43.
Li J P, Yan J W, Xu X Q, et al. Analysis of quantity traceability method of mass flow controller dynamic gas distribution device [J]. Industrial Measurement, 2019, 29 (1): 40-43.
[3]胡红红, 师树恒, 陈富强. 基于质量流量控制器的动态配气系统设计 [J]. 自动化与仪表, 2013, 28 (4): 14-16.
Hu H H, Shi S H, Chen F Q. Design of dynamic gas distribution system based on mass flow controller [J]. Automation & instrumentation, 2013, 28 (4): 14-16.
[4]Kim M E, Kim Y D, Kang J H, et al. Development of traceable precision dynamic dilution method to generate dimethyl sulphide gas mixtures at sub-nanomole per mole levels for ambient measurement [J]. Talanta, 2016, 150: 516-524.
[5]李长武, 陈曹浪, 张斌, 等. 基于临界流喷嘴动态气体稀释装置校准方法研究 [J]. 计量技术, 2018, (5): 32-36.
Li C W, Chen C L, Zhang B, et al. Research on calibration method of dynamic gas dilution device based on critical flow nozzle [J]. Measurement Technique, 2018, (5): 32-36.
[6]江信海. 基于质量流量控制器的智能配气仪及多态配气平台设计开发 [J]. 电子世界, 2018, (19): 144-145.
Jiang X H. Design and development of intelligent gas distribution instrument and multi-state gas distribution platform based on mass flow controller [J]. Electronics World, 2018, (19): 144-145.
[7]胡树国, 杨圣辉, 吴海, 等. 稀释法发生低含量硫化氢气体方法的研究 [C]//全国气体标准化会议. 中国,成都, 2010.
[8]李剑, 王德发, 夏春, 等. 用于低浓度NO2精确测量的傅里叶变换红外光谱系统研究 [J]. 计量学报, 2019, 40 (3): 517-521.
Li J, Wang D F, Xia C, et al. Research on a FTIR System for Accurate Measurement of Low Concentration NO2 [J]. Acta Metrologica Sinica, 2019, 40 (3): 517-521.
[9]宋笑明, 朱茜, 孔小平, 等.气体稀释装置在气体检定中的应用 [J].中国计量, 2017, (2): 121-123.
Song X M, Zhu Q, Kong X P, et al. Application of gas dilution device in gas verification [J]. China Metrology, 2017, (2): 121-123.
[10]李博, 陆进宇, 赵迎晨, 等.标准气体稀释装置校准方法 [J].化学分析计量, 2018, 27 (5): 114-117.
Li B, Lu J Y, Zhao Y C, et al. Calibration method for the dilution device of the reference gas [J]. Chemical Analysis and Meterage, 2018, 27 (5): 114-117.
[11]潘一廷, 张国城, 杨振琪, 等.环境空气监测系统中气体稀释装置的性能比较 [J].计量技术, 2019, (11): 52-56.
Pan Y T, Zhang G C, Yang Z Q, et al. Performance comparison of gas dilution device in ambient air monitoring system [J]. Measurement Technique, 2019, (11): 52-56.
[12]王婧娜, 刘志伟, 严蕊, 等.基于质量流量控制器的高精密配气系统 [J].化工自动化及仪表, 2016, 43 (3): 277-279.
Wang J N, Liu Z W, Yan R, et al. High precision gas distribution system based on mass flow controller [J]. Control and Instruments in Chemical Industry, 2016, 43 (3): 277-279.
[13]徐浩然, 徐科军, 刘文, 等.科氏质量流量计中全数字驱动技术 [J].计量学报, 2020, 41 (11): 1370-1379.
Xu H R, Xu K J, Liu W, et al. All-Digital Drive Technology in Coriolis Mass Flowmeter [J]. Acta Metrologica Sinica, 2020, 41 (11): 1370-1379.
[14]曲宝军, 刘原勇.基于流量控制的两级动态配气系统的研究 [J].山东理工大学学报 (自然科学版), 2016, 30 (5): 29-31+35.
Qu B J, Liu Y Y. Study on a low concentration two level dynamic gas distribution [J]. Journal of Shandong University of Technology (Natural Science Edition), 2016, 30 (5): 29-31+35.
[15]周泽义, 盖良京, 梁建平.标准气体静态容量法配气方法研究 [J].计量学报, 2003, 24(3): 236-239.
Zhou Z Y, Gai L J, Liang J P. Study of calibration gases prepared by static volumetric method [J]. Acta Metrologica Sinica, 2003, 24(3): 236-239.
[16]赵建华, 兰华永, 陈滋健, 等.基于质量流量控制器的多组分动态配气系统研究 [J].自动化仪表, 2008, (2): 44-48.
Zhao J H, Lan H Y, Chen Z J, et al. Research on the Dynamic Multiple Gases Distributing System Based on Mass Flow Controller [J]. Process Automation Instru-mentation, 2008,(2): 44-48.
[17]Brewer P J, Miarro M D, Meane E A, et al. A high accuracy dilution system for generating low concentration reference standards of reactive gases [J]. Measurement, 2014, 47:607-612.
[18]王东丽, 陈传岭, 朱茜, 等.便携式智能气体配气装置的设计 [J].计量技术, 2013, (6): 44-47.
Wang D L, Chen C L, Zhu Q, et al. Design of portable intelligent gas distributor [J]. Measurement Technique, 2013, (6): 44-47.
[19]张守明.动态稀释法配制标准气体在气体分析仪器及气体检测报警器检定中的应用 [J].中国计量, 2008, (11): 75-76.
Zhang S M. Application of standard gas prepared by dynamic dilution method in verification of gas analysis instrument and gas detection alarm [J]. China Metrology, 2008, (11): 75-76. |
|
|
|