The Research on the Superconducting Films for X-ray Superconducting Transition Edge Sensors
JIA E1, LI Wan2, HU Jiahao2, BAI Haijun1, CHEN Jian3, XU Xiaolong3, GUO Siming3, SUN Tianbao3, ZHAO Xiaobo3, LI Jinjin3, WANG Xueshen3
1.College of Information Engineering, Shenyang University of Chemical Technology, Shenyang, Liaoning 110142, China
2.College of Physics, Sichuan University, Chengdu, Sichuan 610064, China
3.Center for Advanced Measurement Science, National Institute of Metrology, Beijing 100029, China
Abstract:Ultra-high vacuum DC magnetron sputtering technology was employed to fabricate both superconducting Mo films and Mo/Au bilayer films, The influence of varying sputtering powers and pressures on film stress, surface roughness, and superconducting transition temperature was investigated. The results for superconducting Mo films revealed a stress range from -421 MPa to 163 MPa, surface roughness below 1 nm, critical temperatures between 1.06 K and 1.10 K. For the Mo/Au films, the stress varied from -38 MPa to 26 MPa, with critical temperatures ranging from 80 mK to 350 mK. The developed Mo/Au bilayer film provides a technical reserve for the development of single-energy X-ray superconducting transition edge sensors(TES).
贾娥, 李万, 胡家昊, 白海军, 陈建, 徐骁龙, 郭思明, 孙天宝, 赵晓波, 李劲劲, 王雪深. X射线超导转变边沿传感器超导薄膜研究[J]. 计量学报, 2025, 46(1): 69-74.
JIA E, LI Wan, HU Jiahao, BAI Haijun, CHEN Jian, XU Xiaolong, GUO Siming, SUN Tianbao, ZHAO Xiaobo, LI Jinjin, WANG Xueshen1.College of Information Engineering, Shenyang University of Chemical Technol. The Research on the Superconducting Films for X-ray Superconducting Transition Edge Sensors. Acta Metrologica Sinica, 2025, 46(1): 69-74.
ALPERT B, BALATA M, BENNETT D, et al. HOLMES: The Electron Capture Decay of 163 Ho to Measure the Electron Neutrino Mass with sub-eV Sensitivity[J]. European Physical Journal C, 2015, 75(3): 1-11.
19
WAKEHAM N A, ADAMS J S, BANDLER S R. Thermal Fluctuation Noise in Mo/Au Superconducting Transition-edge Sensor Microcalorimeters[J]. Applied Physics Letters, 2019, 125(16): 164503.
3
GALER S, HAO L, GALLOP J C, et al. Design Concept for a Novel SQUID-based Microdosemeter[J]. Radiation Protection Dosimetry, 2011, 143(2-4): 427-431.
13
LÜ Y, HUANG H, YOU T, et al. Realization of Precise Tuning the Superconducting Properties of Mn-Doped Al Films for Transition Edge Sensors[J]. Journal of Low Temperature Physics, 2021, 202(2): 71-82.
23
TASKINEN L J, MAASILTA I J. Improving the Performance of Hot-electron Bolometers and Solid State Coolers with Disordered Alloys[J]. Applied Physics Letters, 2006, 89(14): 143-511.
5
AVELLA A, BRIDG G, DEGIOVANNI I P, et al. Self Consistent, Absolute Calibration Technique for Photon Number Resolving Detectors[J]. Optics Express, 2011, 19(23): 249-257.
15
LEVICHEV M Y, BUKHAROV N N, PETROV Y V, et al. The Proximity and Josephson Effects in Niobium Nitride-Aluminum Bilayers[J]. Physical of the Solid State, 2019, 61(9): 1544-1548.
25
王振宇, 曾九孙, 高鹤, 等. 远程靶基距Nb/Al-AlOx/Nb约瑟夫森结薄膜溅射制备技术研究[J]. 计量学报, 2023, 44(9): 1333-1338. WANG Z Y, ZENG J S, GAO H, et al. Fabrication of Nb/Al-AlOx/Nb Josephson Junction Films by a Sputtering Process with a Long Target-substrate Distance[J]. Acta Metrologica Sinica, 2023, 44(9): 1333-1338.
2
HAO L, GALLOP J C, GARDINER C, et al. Inductive Superconducting Transition-edge Detector for Single-photon and Macro-molecule Detection[J]. Superconductor Science and Technology, 2003, 16(12): 1479-1482.
12
OHNO M, TAKAHASHI H, FUKUDA D, et al. Development of a Pixellated Ir-TES for a Large Format TES Array[J]. Nuclear Instruments & Methods in Physics Research Section A-accelerators Spectrometers Detectors and Associated Equipment, 2004, 520(1-3): 414-416.
22
DEIKER S W, DORIESE W, HILTON G C, et al. Superconducting Transition Edge Sensor Using Dilute AlMn Alloys[J]. Applied Physics Letters, 2004, 85(11): 2137-2139.
8
LIN S K. Research Progress of Soft X-ray Analysing Crystals[J]. Journal of Synthetic Crystals, 2012, 41(1): 204-209.
18
XU X, RAJTERI M, LI J, et al. Investigation of Ti/Au Transition-Edge Sensors for Single-Photon Detection [J]. Journal of Low Temperature Physics, 2022, 209(3): 372-378.
4
GALLOP J, COX D, HAO L, et al. Nanobridge SQUIDs as Calorimetric Inductive Particle Detectors[J]. Superconductor Science and Technology, 2015, 28(8): 084002.
6
LITA A E, MILLER A J, NAM S W. Counting Near-infrared Single-photons with 95% Efficiency[J]. Optics Express, 2008, 16(5): 3032-3040.
16
MaRTINIS J M, HILTON G C, IRWIN K D, et al. Calculation of Tc in a Normal-superconductor Bilayer Using the Microscopic-based Usadel Theory[J]. Nuclear Instruments and Methods in Physics Research A, 2000, 444(1-2): 23-27.
26
WANG Y R, LIANG Y J, DING J, et al. Characterizing the Stress and Electrical Properties of Superconducting Molybdenum Films[J]. Superconductor Science and Technology, 2023, 35(2): 025008.
7
马爱文, 曲兴华. SI基本单位量子化重新定义及其意义[J]. 计量学报, 2020, 41(2): 129-133. MA A W, QU X H. The Quantized Redefinition of the SI and Its Signification[J]. Acta Metrologica Sinica, 2020, 41(2): 129-133.
17
OLSEN J, KIRK E C, THOMESEN K, et al. First Steps Towards Small Arrays of Mo/Au Microcalorimeters[J]. Nuclear Instruments and Methods in Physics Research A, 2000, 444(1-2): 253-256.
1
刘贤文, 徐骁龙, 李劲劲, 等. TES用超导薄膜制备及特性研究[J]. 计量学报, 2021, 42(2): 184-188. LIU X W, XU X L, LI J J, et al. Deposition and Characterization of Thin Films for Superconducting Transition Edge Sensor[J]. Acta Metrologica Sinica, 2021, 42(2): 184-188.
11
IRWIN K D. An Application of Electrothermal Feedback for High Resolution Cryogenic Particle Detection[J]. Applied Physical Letters, 1995, 66(15): 1998-2000.
21
POBES C, FÀBREGA L, CAMÓN A, et al. Development of Cryogenic X-ray Detectors Based on Mo/Au Transition Edge Sensors[J]. IEEE Transactions on Applied Superconductivity, 2017, 27(4): 1-5.
10
DEIKER S W, CHERVENAK J A, HILTON G C, et al. Development of Arrays of TES X-ray Detectors[J]. SPIE Optics + Photonics, 2000, 4140(1): 360-366.
20
MINIUSSI A R, ADAMS J S, BANDLER S R, et al. Performance of an X-ray Microcalorimeter with a 240 μm Absorber and a 50 μm TES Bilayer[J]. Journal of Low Temperature Physics, 2018, 193(9): 337-343.
14
YU Q, ZHANG Y F, ZHANG C H, et al. Fabrication and Characterization of Al-Mn Superconducting Films for Applications in TES Bolometers[J]. Chinese Physics B, 2021, 30(7): 077402.
24
WANG H B, LÜ Y, GAO B, et al. Transition-edge Sensors Using Mo/Au/Au Tri-layer Films[J]. Chinese Physics B, 2023, 32(2): 028501.