1.Changzhou Institute of Inspection Testing Standardization and Certification, Changzhou, Jiangsu 213164, China
2.National Institute of Metrology, Beijing 100029, China
Abstract:On the basis of Hammerschmidt's establishment of THB theory, the analytical model and correction model of thermal conductivity under constant input current mode were improved, and the structure design and simulation verification of THB measurement sensors were carried out. An experimental setup and system with a measurement range of 0.01~150W/(m·K) were constructed, and the corrected model was verified through measurement. Seven kinds of solid materials such as polystyrene, PMMA and steel 45 were measured by using the experimental device.The uncertainty of the measurement results was evaluated and compared with the measurement results of different instruments. The experimental results show that the measurement repeatability of the experimental device is better than 1.7%, the relative deviation from the reference value is within ± 5%, and the relative expanded uncertainty of the measurement results is Urel=2.94%(k=2).
ZHOU Y, LIN H, FENG X J, et al. Research the Progresses on Measurement of Thermal Conductivity of Graphene and Graphenes Composites [J]. Acta Metrologica Sinica, 2020, 41(2): 159-169.
YU F, ZHANG X X. Experimental investigation on the thermal conductivity measurement of materials with hot-strip Method [J]. Acta Metrologica Sinica, 2005, 26(1): 27-29.
[9]
GUSTAVSSON M, KARAWACKI E, GUSTAFSSON S E. Thermal conductivity, thermal diffusivity, and specific heat of thin samples from transient measurements with hot disk sensors [J]. Review of Scientific Instruments, 1994, 65(12): 3856-3859.
[10]
PARKER W J, JENKINS R J, BUTLER C P, et al. Flash method of determining thermal diffusivity, heat capacity, and thermal conductivity [J]. Journal of Applied Physic, 1961, 32(9): 1679-1684.
HAMMERSCHMIDT U, MEIER V. New transient hot-bridge sensor to measure thermal conductivity, thermal diffusivity, and volumetric specific heat [J]. International Journal of Thermophysics, 2006, 27(3): 840-865.
CAI J, LIN H, ZHANG J T. Research on relationships between thermal conductivity changes of thermal insulation materials and relative humidity [J]. Building Science, 2013, 29(6): 67-72.
[17]
SVETOZR M, Peter D. Stepwise and pulse transient methods of thermophysical parameters measurement [J]. International Journal of Thermophysics, 2016, 37(12): 114.
JIN T Q. The precise determination of quartz thermal conductivity [J]. Journal of Jilin Institute of Technology, 1991, 12(1): 39-42.
GUSTAFSSON S E, KARAWACKI E, KHAN M N. Transient hot-strip method for simultaneously measuring thermal conductivity and thermal diffusivity of solids and fluids [J]. Journal of Physics D: Applied Physics, 1979, 12(9): 1411-1421.
[15]
精密电阻合金电阻温度系数测试方法:GB/T 618-2005 [S].
HUANG S Y,WEI C X,ZHENG L H. Investigation of the Steady State Method for Thermal Conductivity Measurement and its Data Processing Method[J]. Acta Metrologica Sinica, 2023, 44(4): 508-513.
CHEN M X,HOU D X,YE S L. Test Method of In-plane Thermal Conductivity of Thin Films Based on Laser Thermal Imaging[J]. Acta Metrologica Sinica, 2024, 45(1): 1-8.
LIU Y,ZHANG J T,WANG J K,et al. Study on Measuring Thermal Conductivity of Materials at High Temperature by Guarded-hot-plate[J]. Acta Metrologica Sinica, 2023, 44(6): 871-877.
GUSTAFSSON S E. Transient plane source techniques for thermal conductivity and thermal diffusivity measurements of solid materials [J]. Review of Scientific Instruments, 1991, 62(3): 797-804.
GAISER J, STRIPF M, HENNING F. Enhanced transient hot bridge method using a finite element analysis [J]. International Journal of Thermophysics, 2019, 40(1): 12.
LI L X, LIU Q J, LIU S C, et al. The measurement of thermal conductivity of solids with transient heat wire method [J]. Acta Metrologica Sinica, 2006, 27(1): 39-42.
PAN J, LIU N, WANG Y G, et al. Data analysis for thermal conductivity measurement using transient hot-wire method [J]. Acta Metrologica Sinica, 2015, 36(4): 384-388.
ZHOU Y, LIN H, FENG X J, et al. Measurement of specific heat capacity of metal materials by CW laser heating method [J]. Acta Metrologica Sinica, 2021, 42(11): 1443-1453.
[13]
MODEL R, STOSCH R, HAMMERSCHMIDT U. Virtual experiment design for the transient hot-bridge sensor [J]. International Journal of Thermophysics, 2007, 28(5): 1447-1460.