Abstract:To improve the accuracy of measuring the viscosity of nitrocellulose by falling ball method and reduce the error caused by the non-uniform movement of small ball within the falling ball distance, an accurate measurement method based on two-segment method and changing falling ball height was proposed. PLC and photoelectric sensors were used to design the experimental device. Test solutions with different viscosities were selected to obtain the timing values of different ball drop heights. The suitable drop heights were obtained by fitting the data. The measurement error of traditional and suitable drop height was compared. Experimental results show that there is a negative correlation between the suitable drop height and the viscosity of the test solution; when the viscosity is greater than 60300mPa·s, the suitable drop height is at the drop pipe orifice; when the viscosity is less than 60300mPa·s, releasing the small ball at the appropriate falling height can reduce the measurement error; the lower the viscosity, the more obvious the effect of error reduction.
Mograne M A, Ferrandis J Y, Laux D. Instrumented test tube for rapid rheological behaviour of liquids estimation[J]. Journal of food engineering, 2019, 247:126-129.
When G H, Teng Z S, Lin H J, et al. A Liquid-level Detection Method for Capillary Viscometer Based on Lagrange Parabolic Interpolation[J]. Acta Metrologica Sinica, 2018, 39 (1):47-51.
Huang N M, Su G D, Li G M. Application of C language in the experiment of measuring liquid viscosity by falling ball method[J]. College physics experiment, 2016, 29(4):82-85.
Yang S J, Teng Z S, Lin H J, et al. Design of Intellectual Viscometer Based on Gravity-capillary [J]. Acta Metrologica Sinica, 2009,30 (2): 130-133.
Zhang J, Zhao X H, Pi J A, et al. Measurement methods and progress of viscosity[J]. China instrumentation, 2018 (4):81-86.
Zhang C, Hou M, Zheng X Y, et al. Application of high temperature falling ball viscometer in the production of polypropylene film for power capacitor[J]. Power capacitor, 2005(2):42-45.
Wei K F, Song S Y, Zhang Z Q. Research on Calculation of Natural Mix Gas Viscosity and Reynolds Number[J]. Acta Metrologica Sinica, 2008, 29(3):248-250.
Cheng Y M. Study on measuring liquid viscosity coefficient by falling ball method[J]. Science and Technology Innovation Herald, 2018, 15 (25):107-109.
He F F, li J S, Wu H B. Discussion on the Effect of the Constructing of Viscosity—temperature Curve in the Rotational Viscometer Field Calibration[J]. Acta Metrologica Sinica, 2017, 38(6A):142-145.
[3]
WJ 47—2006硝化棉试验方法粘度黏度计法[S]. 2006.
[10]
李长青. 涂料用硝化棉安定性处理研究[D]. 西安:西北大学, 2017.
Liu Q, Wang H L, Zhang Y, et al. To explore the best experimental conditions and error correction of falling ball method viscosity coefficient experiment[J]. College physics experiment, 2018, 31 (2):103-105.
[7]
Akhlis I, Syaifurrozaq M, Sugiyanto, et al. The determination of fluid viscosity using tracker-assisted falling ball viscosimeter[J]. Journal of Physics Conference Series, 2020, 1567:042102.