Abstract:In order to improve the calibration accuracy of viscometer in non-standard environment laboratory, the viscosity-temperature characteristics of refined petroleum products and refined methylsilicone oil standard viscosity liquids were systematically studied according to experimentally certified viscosity-temperature data. The Walther equation and Arrhenius equation were selected and optimized, and then the kinematic viscosity-temperature correction method of refined petroleum products standard viscosity liquids and the dynamic viscosity-temperature correction method of refined methylsilicone oil standard viscosity liquids were established with the certified values of 20℃ and 25℃ as the reference point. The results show that the maximum deviation between the calculated value and the certified value is 0.65%. The viscosity-temperature correction method used in the calibration of working viscometer is feasible to a certain extent, more accurate viscosity temperature correction in non-standard environment laboratory is realized.
[1] 黄孟孟. 非牛顿流体黏度计量标准研制[D]. 北京: 北京化工大学, 2017.
[2] 邵鸿飞, 高岩立, 任万杰, 等. 溶液型非牛顿流体黏度标准物质的研制[J]. 化学分析计量, 2019, 28(1): 6-8.
Shao H F, Gao Y L, Ren W J, et al. Preparation of viscosity standard reference materials for solution-type non-newtonian fluid[J]. Chemical Analysis and Meterage, 2019, 28(1): 6-8.
[3] 梁秀丽, 张坤, 荀其宁, 等. 血液黏度计校准用标准物质的研制[J]. 计量与测试技术, 2015, 42(7): 53-55.
Liang X L, Zhang K, Xun Q N, et al. The development of blood viscosity meter calibration standard material[J]. Metrology & Measurement Technique, 2015, 42(7): 53-55.
[4] 王星, 潘义, 张鹏辉, 等. 黏度标准物质研制[J]. 中国测试, 2015, 41(5): 5-8.
Wang X, Pan Y, Zhang P H, et al. Development of reference materials of viscosity[J]. China Measurement & Test, 2015, 41(5): 5-8.
[5] 何飞飞, 李劲松, 吴鸿宾. 粘温曲线的建立对旋转粘度计现场校准作用的探讨[J]. 计量学报, 2017, 38(S1): 142-145.
He F F, Li J S, Wu H B. Discussion on the effect of the constructing of viscosity-temperature curve in the rotational viscometer field calibration[J]. Acta Metrologica Sinica, 2017, 38(S1): 142-145.
[6] 马敬东. 粘度测量中的温度修正及其应用[J]. 上海计量测试, 2005, 32(2): 31-32.
Ma J D. Temperature correction in viscosity measurement and its application[J]. Shanghai Measurementand Testing, 2005, 32(2): 31-32.
[7] 刘元俊. 二级标准粘度液定值的不确定度评定[J]. 化学分析计量, 2004, 13(2): 10-13.
Liu Y J. Evaluation of the uncertainty of measurement of secondary standard viscosity liquids[J]. Chemical Analysis and Meterage, 2004, 13(2): 10-13.
[8] 付欣艳. 标准粘度液测量结果不确定度分析及评定[J]. 计量与测试技术, 2010, 37(5): 62-64.
Fu X Y. The analysis and evaluation of uncertainly in measurement on standard liquids of viscosity[J]. Metrology & Measurement Technique, 2010, 37(5): 62-64.
[9] 宋健. 标准毛细管黏度计测量黏度液的不确定度评定[J]. 计量与测试技术, 2008, 35(10): 45-46.
Song J. Evaluation of uncertainty f or measuring viscosity l iquid by standard capillary viscometer[J]. Metrology & Measurement Technique, 2008, 35(10): 45-46.
[10] 王松岭. 流体力学[M]. 北京: 中国电力出版社, 2007: 26-28.
[11] Singh A K, Mukherjee P S, Mishra N M. Interrelationship among viscosity, temperature and age of lubricant[J]. Industrial Lubrication and Tribology, 2006, 58(1): 50-55.
[12] Namburu P K, Kulkami D P, Misra D, et al. Viscosity of copper oxide nanoparticles dispersed in ethylene glycol and water mixture[J]. Experimental Thermal and Fluid Science, 2007, 32(2): 397-402.
[13] Valeri D, Meirelles A J A. Viscosities of fatty acids, triglycerides, and their binary mixtures[J]. Journal of the American Oil Chemists Society, 1997, 74(10): 1221-1226.
[14] Noureddini H, Teoh B C, Clements L D. Viscosities of vegetable oils and fatty acids[J]. Journal of the American Oil Chemists Society, 1992, 69(12): 1189-1191.
[15] Serrano-López R, Fradera J, Cuesta-López S. Molten salts database for energy applications[J]. Chemical Engineering & Processing Process Intensification, 2013, 73(7): 87-102.
[16] Monnery W D, Svrcek W Y, Mehrotra A K. Viscosity: A critical review of practical predictive and correlative methods[J]. Canadian Journal of Chemical Engineering, 1995, 73(1): 3-40.
[17] Yaws C L, Lin X Y, Li B. Calculate viscosities for 355 liquids[J]. Chemical Engineering, 1994, 101(4): 119.
[18] Kulkarni D P, Das D K, Chukwu G A. Temperature dependent rheological property of copper oxide nanoparticles suspension (nanofluid)[J]. Journal of Nanoscience & Nanotechnology, 2006, 6(4): 1150-1154.
[19] Stanciu I. Rheological properties of mineral oil[J]. Journal of Science and Arts, 2011, 4(17): 487-490.
[20] Aworanti O A, Agarry S E, Ajani A O. A laboratory study of the effect of temperature on densities and viscosities of binary and ternary blends of soybean oil[J]. Soy Biodiesel and Petroleum Diesel Oil, 2012, 2(4): 444-452.
[21] 王志芳, 刘逸飞, 傅行军, 等. 润滑油黏温特性实验研究[J]. 润滑与密封, 2016, 41(4): 24-28.
Wang Z F, Liu Y F, Fu X J, et al. Experiment study on viscosity-temperature correlation of lubricating oils[J]. Lubrication Engineering, 2016, 41(4): 24-28.
[22] 王燕霜, 承军伟. 航天轴承润滑油黏温特性及流变特性试验分析[J]. 轴承, 2015, 432(11): 39-41.
Wang Y S, Cheng J W. Experimental analysis on viscosity-temperature characteristic and rheological behavior of lubricating oils for space bearings[J]. Bearing, 2015, 432(11): 39-41.
[23] 王颖文, 张欣, 孙建平, 等. -38. 8344~156. 5985℃温区温标偏差方程外推和内插研究[J]. 计量学报, 2018, 39(6): 816-821.
Wang Y W, Zhang X, Sun J P, et al. Research on extrapolation and interpolation of temperature scale deviation equation over the temperature -38.8344~156.5985℃[J]. Acta Metrologica Sinica, 2018, 39(6): 816-821.
[24] 刘园园, 杨健, 赵希勇, 等. GUM法和MCM法评定测量不确定度对比分析[J]. 计量学报, 2018, 39(1): 135-139.
Liu Y Y, Yang J, Zhao X Y, et al. Comparative analysis of uncertainty measurement evaluation with GUM and MCM[J]. Acta Metrologica Sinica, 2018, 39(1): 135-139.
[25] 陈凌峰. 抽样引起的测量不确定度评定[J]. 计量学报, 2020, 41(7): 891-896.
Chen L F. Evaluating the Sampling Contribution to the Measurement Uncertainty[J]. Acta Metrologica Sinica, 2020, 41(7): 891-896.
[26] 陈凌峰. 标准不确定度A类评定中极差法的深入讨论[J]. 计量学报, 2019, 40(2): 347-352.
Chen L F. The Further Discussion of the Range Method in the Type AEvaluation of Sstandard Uncertainty[J]. Acta Metrologica Sinica, 2019, 40(2): 347-352.
[27] 叶德培. 一级注册计量师基础知识及专业实务:4版[M]. 北京:中国质检出版社, 2017: 333-334.