微型双温度固定点容器研制

曾佳旭,潘江,孙建平,杨月,朱天梦,王成科

计量学报 ›› 2021, Vol. 42 ›› Issue (4) : 458-462.

PDF(1605 KB)
PDF(1605 KB)
计量学报 ›› 2021, Vol. 42 ›› Issue (4) : 458-462. DOI: 10.3969/j.issn.1000-1158.2021.04.09
热学计量

微型双温度固定点容器研制

  • 曾佳旭1,潘江1,孙建平2,杨月1,朱天梦1,王成科1
作者信息 +

Development of Miniature Double Temperature Fixed Point Cell

  • ZENG Jia-xu1,PAN Jiang1,SUN Jian-ping2,YANG Yue1,ZHU Tian-meng1,WANG Cheng-ke1
Author information +
文章历史 +

摘要

基准固定点传递技术应用于现场温度校准已成为提高工业温度测量水平的一种重要途径。采用多孔石墨坩埚半包围结构,内部对称填充了高纯铟(In)和锡(Sn)2种金属,研制了一种应用于现场校准的微型双温度固定点容器。实验结果表明,In点熔化温坪持续时间约为2 h,Sn点熔化温坪持续时间约为3 h,In和Sn的温坪复现的扩展不确定度分别为4.0 mK 和4.4 mK(k=2),可满足工业现场对精密铂电阻温度计的校准需求。

Abstract

Applying the fixed point transfer technology to on-site temperature calibration has become an important way to improve the industrial temperature measurement level. A miniature dual temperature fixed point for field calibration was developed. The fixed point adopted a porous graphite crucible and a semi-enclosed structure filled with two metals, indium and tin. Experimental results showed, at indium point, the temperature plateau curve lasted about 2 hours, and at tin point, the temperature plateau curve lasted about 3 hours. The extended uncertainty reproduced in temperature plateau curve of In was 4.0mK (k=2), and Sn was 4.4mK (k=2). Therefore, the miniature double temperature fixed point device could meet the calibration requirements of precision platinum resistance thermometers in industrial field.

关键词

计量学 / 微型固定点容器 / 铟点 / 锡点 / 现场校准;铂电阻温度计

Key words

metrology;mini fixed point cell;indium point / tin point / field calibration;platinum resistance thermometer

引用本文

导出引用
曾佳旭,潘江,孙建平,杨月,朱天梦,王成科. 微型双温度固定点容器研制[J]. 计量学报. 2021, 42(4): 458-462 https://doi.org/10.3969/j.issn.1000-1158.2021.04.09
ZENG Jia-xu,PAN Jiang,SUN Jian-ping,YANG Yue,ZHU Tian-meng,WANG Cheng-ke. Development of Miniature Double Temperature Fixed Point Cell[J]. Acta Metrologica Sinica. 2021, 42(4): 458-462 https://doi.org/10.3969/j.issn.1000-1158.2021.04.09
中图分类号: TB942   

参考文献

[1]Preston-Thomas H,Quinn T J.The International Temperature Scale of 1990(ITS-90)[J]. Ibid, 1990, 27(1): 3-10.
[2]曾凡超,曾兵,孙建平,等. 基于微型Ga-Sn共晶点的精密铂电阻温度计现场标定[J]. 计量学报, 2015, 36 (6A): 28-31.
Zeng F C, Zeng B, Sun J P, et al. Precision Platinum Resistance Thermometer inthe Field Calibration Based on Miniature Ga-Sn Eutectic Point[J]. Acta Metrologica Sinica, 2015, 36(6A): 28-31.
[3]张洁静. 我国工业温度计量发展状况概述[J]. 中国科技纵横, 2014, (20): 58-58.
[4]张永良,雍海玉,张富余,等. 高精度数字温度装置替代水银温度计的研究与应用[J]. 机械研究与应用, 2017, 30(1): 124-126.
Zhang Y L, Yong H Y, Zhang F Y, et al. Research and Application of High Accuracy Digital Temperature Apparatus Instead of Mercury Thermometer[J]. Mechanical Research & Application, 2017, 30(1): 124-126.
[5]Monalisa R E, Young H L, Yong G K. Fabrication of a mini multi-fixed-point cell for the calibration of industrial platinum resistance thermometers[J]. Measurement Science and Technology, 2017, 28(7): 075007.
[6]Marin S, Hohmann M, Schalles M, et al. Insert with a multiple fixed-point cell for a dry block calibrator[J]. Technisches Messen: Sensoren, Gerate, Systeme, 2015, 82(7/8): 402-410.
[7]刁福广,蔡晋辉,孙建平,等. Ga-In-Sn微型共晶点相变特性研究[J]. 计量学报, 2019, 40(3): 421-426.
Diao F G,Cai J H,Sun J P,et al.  Study on Phase Transition Characteristic of Mini Ga-In-Sn Eutectic Fixed Point[J]. Acta Metrologica Sinica, 2019, 40(3): 421-426.
[8]李訏谟,赵明坚,陈德明. 新一代的温度固定点[J]. 中国测试技术, 2005, 31(1): 6-9.
Li Y M, Zhao M J, Chen D M. New generation of fixed points[J]. China Measurkement Technology, 2005, 31(1): 6-9.
[9]孙建平. 超微量杂质对锌凝固点相变温度影响的研究进展[D]. 北京:北京科技大学,2013.
[10]Pearce J V, Ogura H, Izuchi M. et al. Evaluation of the Pd-C eutectic fixed point and the Pt/Pd thermocouple[J]. Metrologia, 2009, 46(5): 473-479.
[11]金志军,邱萍,孙建平,等. 新型锡、锌固定点炉的研制[J]. 计量学报, 2007, 28 (z1): 28-30.
Jin Z J, Qu P, Sun J P, et al. A New-fashioned Freezing Points Furnace for Realization of Zinc and Tin Freezing Points[J]. Acta Metrologica Sinica, 2007, 28 (z1): 28-30.
[12]武鑫财,孙建平,张连水,等. 便携式锡凝固点复现技术研究[J]. 计量技术, 2012, (12): 53-56.
[13]孙建平,陈炜,邱萍,等. 新型镓熔点自动复现装置[J]. 计量学报, 2013, 34 (2): 134-137.
Sun J P, Chen W, Qiu P, et al. New Automatic Apparatus of the Melting Point of Gallium[J]. Acta Metrologica Sinica, 2013, 34 (2): 134-137.
[14]李利峰, 李锐, 闫小克, 等. 镓熔点温坪复现研究[J]. 计量学报, 2020, 41(4): 419-424.
Li L F, Li R, Yan X K, et al. Study on the Realization of Gallium Melting Point Plateau[J].Acta Metrologica Sinica, 2020, 41(4): 419-424.
[15]Yuan Z D, Wang T J, Lu X F, et al. T90 Measurement of Co-C, Pt-C, and Re-C High-Temperature Fixed Points at the NIM[J]. International Journal of Thermophysics, 2011, 32(7): 1744-1752.
[16]Kawamura Y, Saito I, Nakano T. Realization of the Triple Point of Hg and Observation of a Large Supercooling Using Small Glass Cell[J]. International Journal of Thermophysics, 2019, 40(8):76.

基金

国家重点研发计划重点专项(2017YFF0206300;2017YFF0206303)

PDF(1605 KB)

Accesses

Citation

Detail

段落导航
相关文章

/