Abstract:Applying the fixed point transfer technology to on-site temperature calibration has become an important way to improve the industrial temperature measurement level. A miniature dual temperature fixed point for field calibration was developed. The fixed point adopted a porous graphite crucible and a semi-enclosed structure filled with two metals, indium and tin. Experimental results showed, at indium point, the temperature plateau curve lasted about 2 hours, and at tin point, the temperature plateau curve lasted about 3 hours. The extended uncertainty reproduced in temperature plateau curve of In was 4.0mK (k=2), and Sn was 4.4mK (k=2). Therefore, the miniature double temperature fixed point device could meet the calibration requirements of precision platinum resistance thermometers in industrial field.
[1]Preston-Thomas H,Quinn T J.The International Temperature Scale of 1990(ITS-90)[J]. Ibid, 1990, 27(1): 3-10.
[2]曾凡超,曾兵,孙建平,等. 基于微型Ga-Sn共晶点的精密铂电阻温度计现场标定[J]. 计量学报, 2015, 36 (6A): 28-31.
Zeng F C, Zeng B, Sun J P, et al. Precision Platinum Resistance Thermometer inthe Field Calibration Based on Miniature Ga-Sn Eutectic Point[J]. Acta Metrologica Sinica, 2015, 36(6A): 28-31.
[3]张洁静. 我国工业温度计量发展状况概述[J]. 中国科技纵横, 2014, (20): 58-58.
[4]张永良,雍海玉,张富余,等. 高精度数字温度装置替代水银温度计的研究与应用[J]. 机械研究与应用, 2017, 30(1): 124-126.
Zhang Y L, Yong H Y, Zhang F Y, et al. Research and Application of High Accuracy Digital Temperature Apparatus Instead of Mercury Thermometer[J]. Mechanical Research & Application, 2017, 30(1): 124-126.
[5]Monalisa R E, Young H L, Yong G K. Fabrication of a mini multi-fixed-point cell for the calibration of industrial platinum resistance thermometers[J]. Measurement Science and Technology, 2017, 28(7): 075007.
[6]Marin S, Hohmann M, Schalles M, et al. Insert with a multiple fixed-point cell for a dry block calibrator[J]. Technisches Messen: Sensoren, Gerate, Systeme, 2015, 82(7/8): 402-410.
[7]刁福广,蔡晋辉,孙建平,等. Ga-In-Sn微型共晶点相变特性研究[J]. 计量学报, 2019, 40(3): 421-426.
Diao F G,Cai J H,Sun J P,et al. Study on Phase Transition Characteristic of Mini Ga-In-Sn Eutectic Fixed Point[J]. Acta Metrologica Sinica, 2019, 40(3): 421-426.
[8]李訏谟,赵明坚,陈德明. 新一代的温度固定点[J]. 中国测试技术, 2005, 31(1): 6-9.
Li Y M, Zhao M J, Chen D M. New generation of fixed points[J]. China Measurkement Technology, 2005, 31(1): 6-9.
[9]孙建平. 超微量杂质对锌凝固点相变温度影响的研究进展[D]. 北京:北京科技大学,2013.
[10]Pearce J V, Ogura H, Izuchi M. et al. Evaluation of the Pd-C eutectic fixed point and the Pt/Pd thermocouple[J]. Metrologia, 2009, 46(5): 473-479.
[11]金志军,邱萍,孙建平,等. 新型锡、锌固定点炉的研制[J]. 计量学报, 2007, 28 (z1): 28-30.
Jin Z J, Qu P, Sun J P, et al. A New-fashioned Freezing Points Furnace for Realization of Zinc and Tin Freezing Points[J]. Acta Metrologica Sinica, 2007, 28 (z1): 28-30.
[12]武鑫财,孙建平,张连水,等. 便携式锡凝固点复现技术研究[J]. 计量技术, 2012, (12): 53-56.
[13]孙建平,陈炜,邱萍,等. 新型镓熔点自动复现装置[J]. 计量学报, 2013, 34 (2): 134-137.
Sun J P, Chen W, Qiu P, et al. New Automatic Apparatus of the Melting Point of Gallium[J]. Acta Metrologica Sinica, 2013, 34 (2): 134-137.
[14]李利峰, 李锐, 闫小克, 等. 镓熔点温坪复现研究[J]. 计量学报, 2020, 41(4): 419-424.
Li L F, Li R, Yan X K, et al. Study on the Realization of Gallium Melting Point Plateau[J].Acta Metrologica Sinica, 2020, 41(4): 419-424.
[15]Yuan Z D, Wang T J, Lu X F, et al. T90 Measurement of Co-C, Pt-C, and Re-C High-Temperature Fixed Points at the NIM[J]. International Journal of Thermophysics, 2011, 32(7): 1744-1752.
[16]Kawamura Y, Saito I, Nakano T. Realization of the Triple Point of Hg and Observation of a Large Supercooling Using Small Glass Cell[J]. International Journal of Thermophysics, 2019, 40(8):76.