微量气体转移技术在重量法制备气体标准物质中的应用

胡树国,王德发,王哲

计量学报 ›› 2013, Vol. 34 ›› Issue (1) : 72-75.

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PDF(977 KB)
计量学报 ›› 2013, Vol. 34 ›› Issue (1) : 72-75. DOI: 10.3969/j.issn.1000-1158.2013.01.16

微量气体转移技术在重量法制备气体标准物质中的应用

  • 胡树国,王德发,王哲
作者信息 +

The Application of Trace Gas Transfer Technique  to Preparing Gas CRMs by Gravimatric Method

  • HU Shu-guo,WANG De-fa,WANG Zhe
Author information +
文章历史 +

摘要

微量气体转移技术是一种新兴技术,具有操作便捷、快速等优点。利用该技术在气体标准物质制备过程中可以保持称量准确度不变的情况下,减少制备步骤,特别适合在目标物的纯物质较少或步骤较多的气体标准物质制备中使用。从原理和操作过程等方面对该技术进行介绍,并通过具体实例来验证了该技术的可靠性。

Abstract

Trace gas transfer technique is a new technique with the advantage of convenience and quickness. It decreases dilution times during the preparation of gas CRMs, while keeping weighing accuracy, specially applied to prepare gas CRMs with lack of component gas or multi-dilution. The theory and operating process of this technique is introduced, furthermore, the reliability is verified by experimental data.

关键词

计量学 / 微量气体转移技术 / 重量法 / 气体标准物质

Key words

Metrology / Trace gas transfer technique / Gravimetric method;  / Gas CRMs

引用本文

导出引用
胡树国,王德发,王哲. 微量气体转移技术在重量法制备气体标准物质中的应用[J]. 计量学报. 2013, 34(1): 72-75 https://doi.org/10.3969/j.issn.1000-1158.2013.01.16
HU Shu-guo,WANG De-fa,WANG Zhe. The Application of Trace Gas Transfer Technique  to Preparing Gas CRMs by Gravimatric Method[J]. Acta Metrologica Sinica. 2013, 34(1): 72-75 https://doi.org/10.3969/j.issn.1000-1158.2013.01.16

参考文献

[1]金美兰,赵建南.标准气体及其应用[M]. 北京:化学工业出版社,2003.
[2]全浩,韩永志.准物质及其应用技术(第2版)[M]. 北京:中国标准出版社,2003.
[3]ISO 6142—2001, Gas analysis-preparation of calibration gas mixture gravimetric-method[S].
[4]Brown A S,Milton M J T,Vargha G M.Gravimetric methods for the preparation of standard gas mixtures[J]. Metrologia, 2011,48(5): R1-R9.
[5]胡树国.高纯甲烷中痕量氮气的标准物质的制备、分析和定值[J].计量技术,2009,(11):22-24.

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